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《【扒一扒】日本高纯球形硅微粉材料生产商》:  作为一种无机非金属矿物功能性粉体材料,硅微粉广泛应用于电子材料、电工绝缘材料、胶黏剂、特种陶瓷、精密铸造、油漆涂料、油墨、硅橡胶等领域。 目前,世界上只有中国、日本、韩国、美国等少数国家具备硅微粉生产能力... 全文 ?

1

3M Scotch-Weld Epoxy Adhesives DP-460&DP-420 TDS

最近经常碰到很多客户咨询常温固化的胶水,其实如果需要常温固化有要求很快速的话,UV胶是一个好选择,但是需要添加专门的设备而且要求粘接物至少要一边是透明以便紫外线的照射。另外比较多的可以用瞬干胶或者厌氧胶产品,当然对粘接方式也同样提出了一些要求。再其次是使用一些溶剂胶水(一般在电子行业不多见,在包装、制鞋等行业非常普遍),但必须要考虑通风以及溶剂的挥发性毒性等问题。以上很多都应该属于非结构性的粘接。而现实中最常用的应该是双组分的粘接剂了,也就是俗称的AB胶,以环氧体系和丙烯酸体系为主,而且这类胶水往往能起到结构粘接的作用(参看《关于结构胶粘剂和非结构胶粘剂》)。而电子行业比较常见的有DEVCON的14167系列,以及3M公司的DP810系列等。最近有个客户咨询3M DP420系列的结构胶粘剂,下载相关TDS资料学习了一下(这里面重点强调了各种粘接材料的表面处理问题),有兴趣的朋友可以下载附件查看:

 

Technical Data                                                                                                        September, 1997

(Supersedes December, 1994)

Product Description          Scotch-Weld™ DP-460 and Scotch-Weld™ DP-420 Epoxy Adhesives are high performance, two-part epoxy adhesives offering outstanding shear and peel adhesion, and very high levels of durability.

Features • High shear strength • Controlled flow
• High peel strength • 60 minute worklife (DP-460 Adhesive)
• Outstanding environmental performance or
• Easy mixing • 20 minute worklife (DP-420 Adhesive)

Typical Uncured

Physical Properties

Note: The following technical information and data should be considered representative or typical only and should not be used for specification purposes.

Product DP-460Adhesive DP-420Adhesive
Viscosity (approx..)                    Base@ 73°F (23°C)                              Accelerator 80,000 cps10,000 cps 80,000 cps10,000 cps
Base Resin                                  Base

Accelerator

epoxy amine

epoxy amine

Color                                               Base

Accelerator

white amber

white amber

Net Weight                                    BaseLbs./Gallon                                   Accelerator

9.4

9.0

9.4

9.2

Mix Ratio (B:A)                            Volume

Weight

2:1

2:0.96

2:1

2:0.98

Worklife, 73°F (23°C)                 20 g mixed

10 g mixed

5 g mixed

60 minutes75 minutes

90 minutes

15 minutes20 minutes

30 minutes

Typical Cured

Thermal Properties

Note: The following technical information and data should be considered representative or typical only and should not be used for specification purposes.

Product DP-460Adhesive

DP-420

Adhesive

PhysicalColor Opaque, off-white Opaque, off-white
Shore D Hardness

75-80

75-80

ThermalCoefficient of Thermal     Below Tg Expansion                       Above Tg (in./in./°C) 59 x 10-6

159 x 10-6

85 x 10-6

147 x 10-6

Thermal Conductivity(btu – ft./ft.2 – hr. – °F) @ 45°C

0.104

0.104

ElectricalDielectric Strength (ASTM D 149) 1100 volts/mil 690 volts/mil
Volume Resistivity (ASTM D 257) 2.4 x 1014 ohm-cm 1.3 x 1014 ohm-cm

 

Handling/Application

Information

Directions for Use

Scotch-Weld™ DP-460 and DP-420 Epoxy Adhesives are supplied in dual syringe plastic Duo-Pak cartridges as part of the 3M EPX™ Applicator System. The Duo-Pak cartridges are supplied in 37 ml, 200 ml and 400 ml configurations. To use the 37 ml cartridge simply insert the Duo-Pak cartridge into the EPX Applicator and start the plunger into the cylinders using light pressure on the trigger. Next, remove the Duo- Pak cartridge cap and expel a small amount of adhesive to be sure both sides of the Duo-Pak cartridge are flowing evenly and freely. If simultaneous mixing of Part A and Part B is desired, attach the EPX mixing nozzle to the Duo-Pak cartridge and begin dispensing the adhesive.

 

With the 200 ml and 400 ml cartridges the nozzle must be attached before dispensing any material to prevent unmixed adhesive from getting into the applicator cartridge holder. A small quantity of material should be discarded until uniform color, consistency of product and even flow is evident.

 

When mixing Part A and Part B manually (Scotch-Weld 460 B/A Epoxy Adhesive or Scotch-Weld 420 B/A Epoxy Adhesive), the components must be mixed in the ratio indicated in the Typical Uncured Properties Section of this Technical Data Sheet (page

1). Complete mixing of the two components is required to obtain optimum properties.

Two-part mixing/proportioning/dispensing equipment is available for intermittent or production line use. These systems are ideal for line uses because of their variable shot size and flow rate characteristics and are adaptable to most applications.

……

 

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3M Liquid Optically Clear Adhesive 2152A TDS

3M™ Liquid Optically Clear Adhesive 2152A

Product Description

3M™ Liquid Optically Clear Adhesive 2152A is a UV curing liquid adhesive. It has good bonding strength to various

display substrates like polycarbonate (PC), acrylic and glass without developing bubbles.

Key Features

• UV curable

• Cures in seconds

• Excellent adhesion to glass, polycarbonate, acrylics, etc

Suggested Light Source Wavelength Ranges

UV Cure: 250-400 nm

Technical Data December, 2008

Recommended Curing Conditions

Option 1: Fusion Systems D bulb (high intensity UV Lamp)

• Power: 500W

• Line speed: 10 feet/minute

• Dose: ~2J/cm2 in UVA region

Option 2: Sylvania 15W 350BL (low intensity UV Lamp)

• Curing Time: 5 min

• Dose: ~2J/cm2 in UVA region

Alternate curing systems may be used, providing they deliver a total dose of ~2J/cm2 in UVA region

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3M Optically Clear Adhesives (Contrast Enhancement Film)

最近开始学习了解手机和触屏上的一些用胶点,其中光学透明胶OCA是一个重要应用点,找了一些资料来慢慢学习! 这份《3M Optically Clear Adhesives (Contrast Enhancement Film)》是在2007年时3M公司就发布的资料,世界级的公司始终走在前面的!主要内容如下:

OCA Product Description
Adhesive Transfer Tape (ATT) Format or Double Coat
ATT = Unsupported adhesive sandwiched between two release liners
Formulated for Optical Applications
– Transparent and non-yellowing
– Bonds well to common display polymers and glass
– Bonds well to printed and coated surfaces
Manufactured for Optical Applications
– Clean room or clean practices to minimize defects
–No gels or voids
–Precision coating for uniform caliper
–Clean room ready packaging

几个专有缩写:

ATT—Adhesive Transfer Tape
CEF—Contrast Enhancement Film
OCA—Optically Clear Adhesive
ASF—Anti-splinter film
HTMF—High Transmission Mirror Film
LOCA—Liquid Optically Clear Adhesive
3M Solutions for Touch

Protective tape 
3M Novec  EGC 1720 Electronic Coating
Anti Splinter Film
High Transmission Mirror Film
Trizact Diamond Tile
Optically Clear Adhesive
Contrast Enhancement Film
8880 Ultra Transparent EMI Film
Double Coated Bonding Tapes 
Anisotropic Conductive Film 
Labels

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3M Plastic Bonding Adhesive 2665

3M™ Plastic Bonding Adhesive 2665
Product Description
3M™ Plastic Bonding Adhesive 2665 is a one-component, moisture curing, urethane adhesive that is applied warm.
This low viscosity adhesive has a long open time and is ideal for bonding plastics. Yields thin glue lines when used
with appropriate equipment.
Features
• 100% solids • High tack
• One component • High strength bonds
• Low viscosity • Bonds a variety of plastics
• Long open time
Typical Uncured Properties
Note: The following technical information and data should be considered representative or typical only and should not be
used for specification purposes.
Application Temperature 230°F (110°C)
Viscosity (@ 230°F/110°C)1 11,000 cps
Color (solid) White/Off-white
Open Time2,4 4 minutes
Set Time3,4 Immediate
1Measured on Brookfield viscometer with Thermosel using spindle #27.
2The bonding range of a 1/16" bead of molten adhesive on a non-metallic substrate.
3The minimum amount of time required between when the bond is made and when it will support a 5 psi tensile load.
4Open times and set times are based on a room temperature environment. High temperatures will lengthen open times and set times while lower environmental
temperatures will shorten open times and set times.
3M™ Plastic Bonding Adhesive 2665
Handling/Application Information
Directions for Use
Apply to clean, dry surfaces. Remove oil, grease and other contaminants by wiping with isopropyl alcohol.* For materials
that are often contaminated with mold release agents, it is recommended that the surface be solvent wiped, abraded and
solvent wiped.* For additional information on surface preparation, see section on Surface Preparation.
After heating to suggested application temperature, apply adequate amount of adhesive on one of the substrates to be
bonded. Join the substrates within the adhesives specified open time and hold the bonded part until the adhesive has
adequately set.
*Note: When using solvents, extinguish all ignition sources, and follow the manufacturer’s precautions and directions for use.
Dispensing Equipment
3M™ Plastic Bonding Adhesive 2665 can be dispensed using either a time-pressure dispenser system with luer-lok needle
tips or a positive displacement or gear metering valve to yield thin glue lines. Please approach your local technical team
for more application support.
Container Sizes Available: 30 ml syringes and 295 ml cartridges.
Cleanup: Allow product to solidify. Remove uncured waxy material (usually within the first 20 minutes after application)
by scraping with a putty knife or similar tool. For cured material, remove by cutting or sanding. Do not use heat or flame
to remove adhesive.
Cure Time: The cure rate will vary depending on air temperature, relative humidity, substrate type and bond line thickness.
Typical Performance Characteristics
Note: The following technical information and data should be considered representative or typical only and should not be
used for specification purposes.
Overlap Shear Strength (psi), tested @ 73°F (23°C), Thermal Shock (TS)* and Temperature/Humidity (TH)**
OLSS (PSI)
Substrate 73°F (23°C) After TS After TH
Polycarbonate 940 1,115 945
ABS 690 565 795
Acrylic 830 715 715
Stainless Steel 465 590 490
PVC 560 NT NT
*Condition for TS: -40° to 85°C, 30 minute dwell for 20 cycles.
**Condition for TH: 68°C/95% RH for 3 days.
NT: Not tested.
(2)
3M™ Plastic Bonding Adhesive 2665
Typical Performance Characteristics (continued)
Note: The following technical information and data should be considered representative or typical only and should not be
used for specification purposes.
Rate of Overlap Shear Strength (psi) Build-up @ 73°F (23°C)
Curing Time % of Ultimate
Substrate (hours) OLSS (PSI) OLSS
Polycarbonate 0.083 60 6.5
0.5 195 20
4.0 400 42
16.0 900 95
24.0 940 100
Test Procedures
A. Overlap Shear Strength
Overlap shear (OLS) strengths were measured on 1" wide 1/2" overlap specimens. These bonds were made individually
using 1" x 4" sample coupons. The thickness of the bond line was controlled with .003 - .006" stainless steel wires.
The thickness of the plastics substrates were 0.125".
All strengths were measured at 73°F (23°C) except where noted. The separation rate of the testing jaws was 2" per
minute.
B. Cure Cycle
All bonds were cured for a minimum period of 7 days at 77°F (25°C)/50% RH before testing. Bonds were prepared
using the suggested surface preparation procedure for the particular substrate tested.
Surface Preparation
Plastic: Wipe with isopropanol soaked cheesecloth.* Allow solvent to evaporate before bonding. For optimal performance,
heptane may be used. Note: 3M™ Plastic Bonding Adhesives are not recommended for bonding untreated polyolefins.
Plastic Contaminated with Mold Release: Wipe with isopropyl alcohol soaked cheesecloth, abrade with fine grit abrasive,
wipe with isopropyl alcohol soaked cheesecloth.* Allow solvent to evaporate before bonding. For optimal performance,
heptane may be used.
Metal: Wipe with Methyl Ethyl Ketone (M.E.K.) soaked cheesecloth, abrade with fine grit abrasive, wipe with M.E.K.
soaked cheesecloth.* Allow solvent to evaporate before bonding.
Glass: Wipe with M.E.K.-soaked cheesecloth.* Allow solvent to evaporate before bonding. Priming may be necessary on
glass if subject part will be subjected to hot/humid conditions.
*Note: When using solvents, extinguish all ignition sources, and follow the manufacturer’s precautions and directions for use.
Storage and Shelf Life
Shelf life is 12 months when stored at 60°F (16°C) to 80°F (27°C), indoors and protected from exposure to moisture.

Safety Information
Warning: hot syringes are a possible burn or explosion hazard.
To insure safe handling of 3M™ Plastic Bonding Adhesive 2665 syringes:
1. Do not remove the aluminum label from the syringe. It is designed to make the temperature of the syringe more uniform.
2. The syringe heater must have an opening sufficient to accommodate easy insertion and removal of the syringe including
the aluminum label.
3. Do not exceed 110°C (230°F) syringe temperature. Failure of the syringe could result.
4. Do not exceed 4.1 Bar (60 p.s.i.) dispensing pressure. Failure of the syringe could result.
5. Remove air pressure from the dispensing unit before removing the syringe from the heater.
6. Use only dry air for dispensing to prevent premature curing of the product.
7. Adhesive dripping is sometimes caused by a cured adhesive skin at the syringe back, and can normally be dislodged using
a probe. It is not necessary to remove the skin, merely breaking the seal to the syringe barrel normally cures the problem.
8. Use gloves and personal protective equipment when handling hot syringes to prevent burns or injury.
Certification/Recognition
MSDS: Refer to Product Label and Material Safety Data Sheet for Health and Safety Information before using this product.
For additional health and safety information, call 1-800-364-3577 or (651) 737-6501.
TSCA: The components of this product are in compliance with the chemical notification requirements of TSCA.
RoHs Complaint/REACH Compliant: 3M™ Plastic Bonding Adhesive 2665 complies with the European Union’s
“Restriction of Hazardous Substances” (RoHs) initiative and with European REACH regulations 2002/95/EC and 2005/618/EC.
For Additional Information
To request additional product information or to arrange for sales assistance, call toll free 1-800-251-8634. Address
correspondence to: 3M, Electronics Markets Materials Division, 3M Center, Building 225-3S-06, St. Paul, MN 55144-
1000. Our fax number is 651-778-4244 or 1-877-369-2923. In Canada, phone: 1-800-364-3577. In Puerto Rico, phone:
1-787-750-3000. In Mexico, phone: 52-70-04-00.
Important Notice
All statements, technical information, and recommendations related to 3M’s products are based on information believed
to be reliable, but the accuracy or completeness is not guaranteed. Before using this product, you must evaluate it and
determine if it is suitable for your intended application. You assume all risks and liability associated with such use.
Any statements related to the product which are not contained in 3M’s current publications, or any contrary statements
contained on your purchase order shall have no force or effect unless expressly agreed upon, in writing, by an authorized
officer of 3M.
Warranty; Limited Remedy; Limited Liability.
This product will be free from defects in material and manufacture at the time of purchase. 3M MAKES NO OTHER
WARRANTIES INCLUDING, BUT NOT LIMITED TO, ANY IMPLIED WARRANTY OF MERCHANTABILITY
OR FITNESS FOR A PARTICULAR PURPOSE. If this product is defective within the warranty period stated above,
your exclusive remedy shall be, at 3M’s option, to replace or repair the 3M product or refund the purchase price of the 3M
product. Except where prohibited by law, 3M will not be liable for any indirect, special, incidental or consequential
loss or damage arising from this 3M product, regardless of the legal theory asserted.

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